Respuesta :
Acetinilide is recrystallized using water as a solvent since it has a much higher solubility in hot water than in cold water. the purified solid will not recrystallize later in the experiment if high amount of hot solvent is added in the beginning. So we need to dissolve the sample in minimum amount of boiling water
What is recrystallizing ?
A purification method called recrystallization is used to get rid of contaminants from a sample. The impure sample is dissolved in an ethanol- or water-based solvent. The material dissolves in the liquid solvent after some brief heating. The solid precipitates out of the solution when the solvent cools down once more, leaving the impurities in the solvent that are still dissolved behind.
Then activated charcoal is added to remove the coloured impurities. After hot film pareshan insoluble impurities are removed. And then cold filtration separates the solid from solution.
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